Purification of Organic Compounds- Complete Handwritten Note
3 views 0 purchase
Course
Chemistry
Institution
This complete handwritten note covers the whole of basic purification techniques, qualitative analysis (detection of elements- C, H, N, S, X(halogens-Cl, Br, I) and P) and quantitative analysis (estimation of elements- C, H, X(halogens- Cl, Br, I), P, N and O.
-lo Se peraba
ImpuYitie
SUdinable orqanic cowpoun
Cam phor.
bexachloro naphnqloneanacene,antraquinone,
onzoie aid,
eane
( ) apvsTALLIGATl0
-A most general me oa t
- |4
poify ooid orqanic com pound
USine a Solvont "1n hich toe eom pound 1s paiincghy
Solble at tempoature but a pvecia bly dubte t bcn
4empat r
e eampund grcadualy Cwystallsa t
from leavina b bind all ne
u) DisWLLATGnN
Ponf Loklqle organic compound TUquid)
typen
(a) Gmple dsillation:
Se perale uolalile CompoUnd tom nen \lobile imponttey
Sepeate too misible iqvid i t consdeae ufîerencQ
bolina pont (>2 6c)
" cslo o fom C6c) aniune Cbp-lB4C)
dueyl ehcy (35O u Toluene ( l l ° )
mDtue
teront te mpe qtey.
e t o uaic la po|se a t
Pindple
bolin poln Wauid \apouI Se
fist Te a r s are
coleetd
Ondensec
(b) fractonal Disilla|in
wusscible Liaui
To Gepeyate two
elone
pe to leum\nity
hati ons
Pansed
e Vapuu
Sas temparcat
clunn
, hng eslumn ol multple su face
(colmn)
cc ) acuv m
Diillatn (Drtllatlon ond a preUre ):
oY
made u bol at loe empaetre boy
Phnciple; A s exkmal pre ssue derrere
(d) Steam istilla thon:
-to arl stea Wol atile and ond 'imide
wit a ey
, o no- nito phenl Sal caldehucle 6rho hydoy aetprn
Tbe iaui naving o-\S
callec steam Molaile Liq
at 100C
S4eam vog he bated '1mpure Sam ple ofstea
Volatile poundl slapouy of stean Valatk
(iqvid wlll
pnncsle A always bals a
The nGrnal
a
components
Condiion wwales volatl Pat.
loecawSe
(i) PIFERENWAL TXTRACI0N
- Done by aqveo medOm
rmxtu
) tc solent wwst be
IwwrsCble wnate.
nan
, " chloro oricnloromnehane
Ae more cdenso an atei
Jater mcible soluont al cannol be sed,, foy Aferontal ox traos
e hanol Calcohols), acetoe, diehel etes
(V) CHPOMAT0aPAPHY
- A Veny gonerGl me hod
Mus moden me thsd
miIte
phase is alowed to moe slouly t n he
Staoney nae 3Yaduly 3t
Seperaleel ver e statñonv hoye Cau Sa
cowUnei'wTa
2-ps
stetiuny tphase
hwmotgraphy
c howutara phy
m)
-Staionmy Pnae = Solicl adsbont (siica sel or e)uini
phase USucll an og <olWon
2x Column chsmologphy i tiin layo chomote py (7<)
u) P a t i o n chromotoaphy
mole pha\e
Hence
ex. Papo chromoto qraphy
seperati,
priiple Diffeyontial adsov ptiun
adsovod an givon ad Soybent
f Different compound
abbod more play adsoens
ike
a) coonnn hiono tu graphy.
can larye Scal Sepa t i o n t co mpondy
Seperetm o Com puundi ccUrs Column ot uds hont
glss e
ue to placod
The moVe
olun, a obile Is alowad t0
adsoybent
calumn. 9ramic
dissolv ed n ne sulvont
wi
The benefits of buying summaries with Stuvia:
Guaranteed quality through customer reviews
Stuvia customers have reviewed more than 700,000 summaries. This how you know that you are buying the best documents.
Quick and easy check-out
You can quickly pay through credit card or Stuvia-credit for the summaries. There is no membership needed.
Focus on what matters
Your fellow students write the study notes themselves, which is why the documents are always reliable and up-to-date. This ensures you quickly get to the core!
Frequently asked questions
What do I get when I buy this document?
You get a PDF, available immediately after your purchase. The purchased document is accessible anytime, anywhere and indefinitely through your profile.
Satisfaction guarantee: how does it work?
Our satisfaction guarantee ensures that you always find a study document that suits you well. You fill out a form, and our customer service team takes care of the rest.
Who am I buying these notes from?
Stuvia is a marketplace, so you are not buying this document from us, but from seller nihalahmedp. Stuvia facilitates payment to the seller.
Will I be stuck with a subscription?
No, you only buy these notes for $5.48. You're not tied to anything after your purchase.
